Acidic and Basic Reagents , Handbook of Reagents for Organic by Hans J. Reich, James H. Rigby

By Hans J. Reich, James H. Rigby

Recognising the severe want for bringing a convenient reference paintings that offers not just with the preferred reagents in synthesis to the laboratory of practicing natural chemists, the editors of the acclaimed 'Encyclopedia of Reagents for natural Synthesis' (EROS) have chosen crucial and helpful reagents hired in modern natural synthesis.

This booklet offers articles at the such a lot primary and flexible reagents for effecting natural ameliorations that have been initially incorporated in EROS. In choosing candidate entries for inclusion during this specific assortment, the editors followed a huge set of standards for outlining what precisely constitutes an acidic or simple reagent.

Each article includes all the info present in EROS in addition to multiplied similar reagents listings. extra new listings of lately released overview articles and monographs are integrated, in addition to appropriate 'Organic Syntheses' tactics that care for both the arrangements or reactions of the featured reagents. This thorough and finished guide can have common attraction.

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C. JACS 1984, 106, 434. 10. Finger, C. S 1970, 541. 11. Bestmann, H. ; Frey, H. LA 1980, 2061. 12. S 1990, 931. 13. Pyne, S. ; Spellmeyer, D. ; Fuchs, P. L. JACS 1982, 104, 5728. 33) (chiral ligand and auxiliary1) Alternate Name: BINOL. Physical Data: mp 208-210°C; [a] 21 +34° (c= 1, THF). Solubility: sol toluene, CH2C12, EtNO2. Form Supplied in: white solid; widely available. 4 The best procedure uses (+)amphetamine as the chiral ligand and provides BINOL in 98% yield and 96% ee. Above 25 °C the CuII/(+)-amphetamine/(S)BINOL complex precipitates while the more soluble CuII/(+)amphetamine/(R)-BINOL complex is slowly transformed into the former complex.

Shteingarts, V. D. JOU 1978, 14, 2069. S 1970, 361. (a) Karpov, V. ; Panteleev, I. ; Platonov, V. E. JOU 1991, 27, 1932. (b) Karpov, V. ; Platonov, V. ; Yakoboson, G. G. IZV 1979, 2082. Taylor, S. ; Martin, J. C. JOC 1987, 52, 4147. Olah, G. ; Tolgyesi, W. ; Kuhn, S. ; Moffatt, M. ; Bastien, I. ; Baker, E. B. JACS 1963, 85, 1328. For reviews, see (a) Olah, G. ; Prakash, G. K. ; Saunders, M. ACR 1983,16,440. (b) Brown, H. C. ACR 1983, 16, 432. (c) Walling, C. ACR 1983, 16, 448. (a) Schleyer, P.

15. ; Schallner, O. AG(E) 1973, 12, 399. (b) Farcasiu, D. CC 1977, 394. 16. (a) Belen'kii, G. ; Savicheva, G. ; German, L. IZV1978, 1433. (b) Belen'kii, G. ; Lur'e, E. ; German, L. S. IZV 1976, 2365. (c) Petrov, V. ; Belen'kii, G. ; German, L. S. IZV 1980, 2117. (d) Karpov, V. ; Mezhenkova, T. ; Platonov, V. ; Yakobson, G. G. JOU 1984, 20, 1220. (e) Petrov, V. ; Belen'kii, G. ; German, L. ; Kurbakova, A. ; Leites, L. A. IZV 1982, 170. (f) Karpov, V. ; Mezhenkova, T. ; Platonov, V. ; Yakobson, G.

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